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Guide · Materials

How to cement e.max crowns and onlays: HF etch and silane

Step-by-step cementation of e.max (IPS e.max CAD) crowns and onlays, with 5% hydrofluoric acid for 20 seconds and silane, and when self-adhesive cement works.

By Equipe técnica Smile Digital LabUpdated 7 min read

Short answer

Cementing e.max (IPS e.max CAD) with a resin cement starts outside the mouth, after try-in: 5% hydrofluoric acid on the intaglio for 20 seconds, then silane for 60 seconds. A crown on a retentive prep can take an adhesive, self-adhesive or conventional cement; onlays, veneers and minimally invasive crowns must be bonded.

Step by step

  1. 01

    Remove the provisional and clean the prep

    Take off the provisional and clean the prep with an oil-free, fluoride-free paste. Ivoclar notes that eugenol temporary cements and peroxide disinfectants interfere with resin cement polymerization.

  2. 02

    Try in the restoration with try-in paste

    Check fit, shade and occlusion with the cement's try-in paste. Go carefully on occlusion: before cementation, the ceramic can fracture. If you adjust, use a fine diamond, light pressure and water cooling, then polish the area.

  3. 03

    Etch with 5% hydrofluoric acid for 20 seconds

    Outside the mouth, cover the intaglio with 5% hydrofluoric acid for 20 seconds, rinse with water spray and dry with oil-free air. If the restoration arrived already etched, clean it with a cleaning paste for 20 seconds instead.

  4. 04

    Apply silane for 60 seconds

    Apply the silane primer to the etched surface, leave it for 60 seconds and disperse with a strong air stream, without pooling. A silane-containing universal adhesive doesn't replace a separate primer.

  5. 05

    Isolate and prepare the tooth for your cement

    For adhesive cementation, relative or absolute isolation is required and the tooth gets the cement's bonding system. For a self-adhesive cement, follow the cement IFU for tooth preparation.

  6. 06

    Seat with the right cement for the restoration

    Seat the restoration, hold it in place and remove the excess at the margins and interproximally before the final cure. Onlays, veneers and minimally invasive crowns go in with adhesive cement only.

  7. 07

    Check the margins, contacts and occlusion

    Floss the contacts, look for excess at the margins and check the occlusion with the restoration cemented.

When can e.max go in with a self-adhesive or conventional cement?

e.max takes a self-adhesive or conventional cement only as a crown or a three-unit bridge on a retentive prep, according to the IPS e.max CAD IFU (Ivoclar, 2026). Veneers, inlays, onlays and minimally invasive crowns must be bonded, and adhesive cementation is also the only option on a non-retentive prep.

IPS e.max CAD restorationadhesiveself-adhesiveconventional
Veneeryesnono
Inlay and onlay, including occlusal veneers and partial crownsyesnono
Minimally invasive crownyesnono
Crownyeson a retentive prepon a retentive prep
Three-unit bridge up to the second premolaryeson a retentive prepon a retentive prep

The same IFU puts more limits on minimally invasive crowns: nothing under 1 mm, composite resin cores only, canine guidance present and never on implants. Minimum thicknesses for each restoration are in monolithic, multilayer zirconia or e.max.

A retentive prep has 10 to 20° of total occlusal convergence and at least 4 mm of occlusocervical height on molars and 3 mm on other teeth. Those are the values in Goodacre and colleagues’ classic review (The Journal of Prosthetic Dentistry, 2001).

Clinically, the cement makes little visible difference. Maroulakos and colleagues’ review (The Journal of Prosthetic Dentistry, 2019) found survival of 83.5% to 100% for bonded lithium disilicate crowns and 98.5% in the single conventionally cemented group, with poor-quality evidence.

What hydrofluoric acid should you use on e.max, and for how long?

e.max (lithium disilicate) is etched with 5% hydrofluoric acid for 20 seconds, according to Ivoclar’s Monobond Plus and Variolink Esthetic LC instructions. Leucite glass-ceramics such as IPS Empress get 60 seconds; lithium disilicate gets only 20.

More time and a stronger acid don’t help. May and colleagues (The Journal of Prosthetic Dentistry, 2022) ran a meta-analysis of lab studies: acid above 4.9% for 20 seconds or longer lowered the flexural strength of lithium disilicate without changing roughness. On feldspathic and leucite ceramics, 5% for 30 to 120 seconds increased roughness with no loss of strength.

Etching happens outside the mouth. Özcan and colleagues’ review (Clinical Oral Investigations, 2012) describes hydrofluoric acid as aggressive to soft tissue, with symptoms that may not show right away, and urges precautions for clinicians who use it chairside.

The IPS e.max CAD IFU also says the restoration must not be blasted with alumina. Air abrasion is the zirconia treatment.

What does silane do on e.max?

Silane is the primer that promotes the bond between etched e.max and the resin cement. In the Monobond Plus IFU, it stays on the etched surface for 60 seconds and is dispersed with a strong air stream; in crowns, without pooling.

A separate primer outperforms a silane-containing universal adhesive. Lima and colleagues’ meta-analysis (The Journal of Prosthetic Dentistry, 2024) pooled 26 lab studies. On lithium disilicate, hydrofluoric acid followed by a ceramic primer bonded better than acid followed by a silane-containing universal adhesive.

There is an alternative to the acid: a self-etching ceramic primer, which etches and silanates from one bottle. In the same meta-analysis, its bond was similar to acid plus silane. Ivoclar describes Monobond Etch & Prime in the Variolink Esthetic LC IFU: scrub for 20 seconds, leave for another 40, then rinse until the green color is gone.

With a self-adhesive cement, silane stays in the protocol. In its RelyX cement pretreatment guide, 3M calls for hydrofluoric acid and silane on glass-ceramics with its self-adhesive cement too.

What do you do when e.max is contaminated at try-in?

Contaminated e.max is cleaned before silane, and how depends on whether it was already etched. A restoration that wasn’t etched is rinsed, dried and etched after try-in, which also cleans the surface. A restoration etched before try-in gets a cleaning paste, per the Variolink Esthetic LC IFU: rinse, apply Ivoclean for 20 seconds, rinse, dry and then prime.

If silane was already on, it goes on again after cleaning, according to the Ivoclean IFU. And if the restoration is contaminated with saliva, blood or water after priming, the Monobond Plus IFU says to repeat the whole treatment.

The cleaning paste has one limit: the Ivoclean IFU contraindicates it on a restoration that has touched a silicone-based material.

How do you cement an e.max onlay?

An e.max onlay can only be bonded: the IPS e.max CAD IFU doesn’t allow self-adhesive or conventional cement for inlays, onlays, occlusal veneers or partial crowns. The Variolink Esthetic LC IFU requires relative or absolute isolation, and the Monobond Plus IFU says not to use the primer without a dry field.

At try-in, Ivoclar asks for care when checking the occlusion of a ceramic restoration that isn’t cemented yet, because it can fracture. Any adjustment is done with a fine diamond at medium speed, light pressure and water cooling, and the adjusted area is polished.

A light-cure-only cement fits a thin onlay. Variolink Esthetic LC is indicated for translucent inlays, onlays and veneers under 2 mm; for a thicker or opaque restoration, Ivoclar doesn’t indicate it.

The studies behind e.max onlays used adhesive cementation, and the numbers are on the e.max or zirconia onlay page.

How does cementing e.max differ from zirconia?

The difference between cementing e.max and zirconia is the intaglio: e.max is etched with hydrofluoric acid and silanated; zirconia is air-abraded with alumina and, for adhesive cementation, primed with MDP.

stepe.max (IPS e.max CAD)zirconia
Intaglio5% hydrofluoric acid for 20 secondsalumina air abrasion
Air abrasionnot to be doneit is the treatment
Primersilane, 60 secondsMDP primer, for adhesive cementation only
Cleaning after try-inetch after try-in, or a cleaning paste if it arrived etchedre-blast or a cleaning paste, no phosphoric acid
Self-adhesive and conventionalcrowns and bridges only, on a retentive prepcrowns and bridges, on a retentive prep

The zirconia steps, including RelyX U200, zinc phosphate and implant crowns, are in how to cement zirconia crowns.

What mistakes compromise e.max cementation?

The mistakes that most compromise e.max cementation are in etching the restoration and in matching the cement to the type of restoration.

mistakewhat happenshow to avoid itsource
Etching longer or with a stronger acid than the IFUlower flexural strength, with no gain in roughness, in vitro5% acid for 20 secondsMay et al., 2022; Ivoclar, Monobond Plus
Swapping silane for a silane-containing universal adhesiveweaker bond to lithium disilicate, in vitroa separate ceramic primerLima et al., 2024
Sandblasting e.maxoutside the manufacturer’s instructionshydrofluoric acid onlyIvoclar, IPS e.max CAD
Self-adhesive or conventional cement on an onlay, veneer or minimally invasive crownoutside the manufacturer’s indicationsadhesive cementationIvoclar, IPS e.max CAD
Cementing without a dry fieldcontamination means repeating the restoration treatmentrelative or absolute isolationIvoclar, Monobond Plus and Variolink Esthetic LC
Eugenol temporary cement or a peroxide disinfectant on the prepresin cement polymerization is inhibited or impairedeugenol-free temporaries and an oil-free cleaning pasteIvoclar, Variolink Esthetic LC
Etching in the mouthsoft-tissue injury from hydrofluoric acidetch outside the mouthÖzcan et al., 2012

What comes from the lab, and what goes on the Rx?

Smile Digital Lab makes e.max restorations from IPS e.max CAD, by Ivoclar, in its own ceramics department in São Paulo, Brazil, stained and glazed by hand. The restoration arrives ready for try-in; etching, silane and cementation happen chairside. Ask the lab whether the intaglio comes etched, because that changes the cleaning after try-in.

On the Rx, include:

  • The cement you plan to use. With a self-adhesive or conventional cement, the restoration has to be a crown on a retentive prep; a minimally invasive crown only exists with adhesive cementation.
  • The stump shade, especially with a metal core or a discolored tooth. Ivoclar says to pick the block by the shade of the prep at its most discolored area.
  • Bruxism. In the IPS e.max CAD IFU, untreated bruxism is a limitation of use, with a splint indicated after placement.

If the space falls short of the material’s minimum thickness, we contact you before milling. We check every case when it arrives and on eight points before it ships. The restorations are on the e.max crown and e.max or zirconia onlay pages, and stump shade in the shade guide.

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Frequently asked questions

Can I cement an e.max crown with a self-adhesive resin cement?

Yes, for crowns and three-unit bridges on a retentive prep: the IPS e.max CAD IFU lists self-adhesive cementation for those. Onlays, veneers and minimally invasive crowns are left out. In its RelyX cement pretreatment guide, 3M still calls for hydrofluoric acid and silane on glass-ceramics with its self-adhesive cement.

Can I use 9% or 10% hydrofluoric acid on e.max?

Ivoclar's instructions call for 5% acid for 20 seconds on lithium disilicate. In a meta-analysis of lab studies (May and colleagues, 2022), acid above 4.9% for 20 seconds or longer lowered the flexural strength of lithium disilicate without increasing roughness. Higher concentrations and longer times are outside the IFU.

Does a silane-containing universal adhesive replace silane?

No, according to Lima and colleagues' meta-analysis (The Journal of Prosthetic Dentistry, 2024): on lithium disilicate, hydrofluoric acid followed by a separate ceramic primer bonded better than acid followed by a silane-containing universal adhesive. A self-etching ceramic primer, which etches and silanates from one bottle, performed about the same as acid plus silane.

Can e.max be sandblasted?

No. The IPS e.max CAD IFU says the restoration must not be blasted with alumina or glass polishing beads. Retention on lithium disilicate comes from hydrofluoric acid; air abrasion is the zirconia treatment.

Sources

  1. IPS e.max CAD — Instructions for Use (Rev. 5, 2026) · Ivoclar Vivadent
  2. Monobond Plus — Instructions for Use (Rev. 0, 2023) · Ivoclar Vivadent
  3. Variolink Esthetic LC — Instructions for Use (Rev. 1, 2025) · Ivoclar Vivadent
  4. Ivoclean — Instructions for Use (Rev. 0, 2025) · Ivoclar Vivadent
  5. 3M RelyX Cements — Material Pretreatment Guide · 3M Oral Care (2020)
  6. Effect of milling, fitting adjustments, and hydrofluoric acid etching on the strength and roughness of CAD-CAM glass-ceramics: a systematic review and meta-analysis · The Journal of Prosthetic Dentistry (May et al., 2022)
  7. Effect of universal adhesives and self-etch ceramic primers on bond strength to glass-ceramics: a systematic review and meta-analysis of in vitro studies · The Journal of Prosthetic Dentistry (Lima et al., 2024)
  8. Effect of cement type on the clinical performance and complications of zirconia and lithium disilicate tooth-supported crowns: a systematic review · The Journal of Prosthetic Dentistry (Maroulakos et al., 2019)
  9. Possible hazardous effects of hydrofluoric acid and recommendations for treatment approach: a review · Clinical Oral Investigations (Özcan et al., 2012)
  10. Tooth preparations for complete crowns: an art form based on scientific principles · The Journal of Prosthetic Dentistry (Goodacre et al., 2001)

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